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Pilot unit for wet-process phosphoric acid

A modular pilot line for comparing phosphate feedstocks and evaluating their processability. The concept links grinding, homogenisation, sulphuric-acid digestion, filtration and test-data assessment.

The whole application matters.

The proposed skid contains a mill, homogenisation tank, agitated reactor and vacuum filter. Adjustable acid dosing, temperature and residence time enable different test conditions. pH, temperature and composition measurements are linked to the controls and recorded in a standard test report.

Scope of the solution

  • Feed preparation and homogenisation, an agitated reactor and chemical pumps.
  • Vacuum filtration separating acid filtrate from gypsum cake.
  • PLC with HMI, operating-data logging and proposed XRF analysis.
  • Frame, drip trays, piping and valves, with basic operating and test documentation.

From operating need to design.

01

Project objective

Obtain comparable data on different ores, acid consumption, phosphorus transfer to the product and filterability of the gypsum by-product.

02

Supply interfaces

Representative ore samples, particle size and analyses of P₂O₅ and accompanying impurities.

03

Engineering output

PFDs, P&IDs, equipment list and instrumentation database.

Inputs that matter.

  • Which ores and composition ranges should be compared?
  • Which test conditions and analytical outputs are required?
  • Should the pilot cover digestion and filtration only, or further acid treatment as well?
  • What requirements apply to relocation, utilities and disposal of by-product streams?
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Outputs and acceptance.

  • PFDs, P&IDs, equipment list and instrumentation database.
  • Operating and maintenance manual, test-report template and acceptance-test plan.
  • Proposed FAT, feedstock validation and SAT, installation supervision and operator training.

The actual scope and acceptance criteria depend on the application and contract.

Concrete configurations and supply scopes.

These examples describe proposed solutions and enquiry requirements. Their parameters belong to the stated project stage; completed supplies are shown separately in the project portfolio.

Preliminary process concept

Project 0878 · 2025 · Middle East

Pilot unit for wet-process phosphoric acid

Pilot capacity target1 t P₂O₅/dayA design target dependent on the composition and processing of the particular ore.
Preliminary reactor configuration2 m³; 7.5 kW agitatorProposed equipment, subject to refinement after testing and balance calculations.
Filtration area2 m²A vacuum belt filter considered in the preliminary design.

Requirement

Obtain comparable data on different ores, acid consumption, phosphorus transfer to the product and filterability of the gypsum by-product.

Proposed solution

The proposed skid contains a mill, homogenisation tank, agitated reactor and vacuum filter. Adjustable acid dosing, temperature and residence time enable different test conditions. pH, temperature and composition measurements are linked to the controls and recorded in a standard test report.

Proposed scope

  • Feed preparation and homogenisation, an agitated reactor and chemical pumps.
  • Vacuum filtration separating acid filtrate from gypsum cake.
  • PLC with HMI, operating-data logging and proposed XRF analysis.
  • Frame, drip trays, piping and valves, with basic operating and test documentation.

The example is based on a preliminary 2025 proposal. Performance, materials, analytical methods and test criteria are verified for the specific feedstock.

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Expertise for this application.

A clear brief.
A practical next step.

Send your drawings, operating parameters or a short description of the change you need. We will review the technical interfaces and propose the next steps towards a quotation, clarifying any missing information with you.

Discuss your requirements ↗Prepare a technical brief →+420 731 771 147info@emkoproject.cz